save data in xtal.evc [Yes]
yes
Created xtal.evc
s01f002.shoe.Z Opened
Trying s01f002.evc
Refl nr [1]
1
Goniostatoffset: ToGoniostatRotZero
1.0000000 0.0000000 0.0000000
0.0000000 0.0000000 -1.0000000 Determinant: 1.000000
0.0000000 1.0000000 0.0000000
SCAN PHI PIXELSIZE 0.15 0.15 DETECTORSIZE 172.5 172.5 Dist 480.0
End-Of-Header
Stored rmat as 1 Cell: 102.8588 102.8587 59.1378 90.000 90.000 120.000 Volume: 541850.2
SetupPolarisation OSMIC W/S=1.0 polar=0.5 pn1=(0.0 1.0 0.0) pn2=(0.0 0.0 1.0) Alpha:0.846899 Mid:0.846899 Mean:0.846899
Lambda:0.846899 AlphaCorrection:0.0 polar:0.5
Neighbour check ON
RMAT000[1] at Goniostat (RotZero)
0.0008068 0.0036088 0.0159178 0.0008068 0.0036088 0.0159178
-0.0111638 -0.0046453 0.0007132 0.0008619 0.0095615 -0.0056614
-0.0008619 -0.0095615 0.0056614 -0.0111638 -0.0046453 0.0007132
Determinant: 0.1845529E-05 0.1845529E-05
Orig: hor=13.41 ver=-89.33 rot=25.0 hkl: 13.41 -89.33 25.0 diff: 0.0 0.0 0.0
beamstopvector -480.0 0.0 0.0 MIDLINE swing=0.0 myrotax 0.0 -50.0 0.0 beamstop=-480.0 0.0 0.0 dethor=172.5 detver=172.5
v -480.0 -50.0 0.0 detvec -480.0 0.0 0.0 f=2.23 beamstop -480.0 0.0 0.0 rax -480.0 -50.0 0.0 from -172.5 0.0 to 172.5 0.0
DurationArc DetectorSmax 0.55 detectorthmax 13.51 generated 125 neighbours tested 26
Frame: 3033.95 3091.9 3099.67 3017.31 2991.25
Theta:5.33 Resolution: 4.56 Chi:-8.5 Duration:1.02
Contour: H(12.84,14.01)=1.16[8] V(-89.73,-88.94)=0.78[5] R(-1.39,0.39)=1.79[2]
Pixels: Peak=62/5.5% Surface=104 Bg=1021
Excluded: 42 HV=28/26.92% I(Ex/Pk)=16.36% I(HV/Pk)=12.89% BadI 4.05%
Background: A=-1.14 B=-1.81 C=3066.05 Sig=77.43 Slope=0.53
Intensity: Hor=148371.09 Ver=150905.73 Rot=154781.0 Plane=154523.27 BgQual=0.04 (peakbg=154471.48)
Shifts:2 H 0.06px 0.01mm V -0.01px 0.0mm rot=-0.11 Frames=2 dxfactor=1.00003 AlphaCorrection: 0.0 0.0 0.0
RotCorrection: 0.0 0.0 0.11
Final Position: 13.42 -89.33 24.89 Integrated Position: 13.42 -89.33 25.0
Rnet=154523.27 Poisson=725.42 (sigBPB=595.46) GarbageSigma=6263.46 Weight=609.68 PQ=253.45 I/Sig=213.01
Corrections: Lorentz:4.6304 Polar:0.9829 LP:0.2197 Incidence:1.0 Final:0.2197
Corrected: Rnet=33952.27 Sigma=159.39 newSigma=1376.22
nr h k l QVP DetH DetV Rot Int sigPois PQ obxXyYzZ
1 15 5 5 13.42 -89.33 24.89 33952.3 1376.2 253.5 ........
Refl nr [2]
\repeat 5 pq20 \wait 5
2 17 -19 8 -88.18 -48.83 25.06 857.5 72.5 11.9 ........
Orig: hor=52.28 ver=66.16 rot=25.0 hkl: 52.28 66.16 25.0 diff: 0.0 0.0 0.0
generated 125 neighbours tested 6
Frame: 3039.87 3027.67 3025.25 3029.2 3021.24
Theta:4.98 Resolution: 4.88 Chi:-38.15 Duration:1.28
Contour: H(51.73,52.82)=1.09[7] V(65.68,66.66)=0.98[7] R(-1.43,0.44)=1.88[2]
Pixels: Peak=62/5.5% Surface=100 Bg=1055
Excluded: 8 HV=1 Rot=2 I(Ex/Pk)=6.85% BadI 7.06%
Background: A=-0.87 B=-0.43 C=3039.4 Sig=61.84 Slope=0.3
Intensity: Hor=18822.43 Ver=18145.85 Rot=15491.33 (2) Plane=18785.87 BgQual=0.19 (peakbg=18773.39)
Shifts:2 H -0.03px 0.0mm V 0.04px 0.01mm rot=0.19 Frames=2 dxfactor=1.00002 AlphaCorrection: 0.0 0.0 0.0
RotCorrection: 0.0 0.0 -0.19
Final Position: 52.28 66.17 25.19 Integrated Position: 52.28 66.17 25.0
Rnet=18785.87 Poisson=505.89 (sigBPB=466.48) GarbageSigma=1325.57 Weight=486.96 PQ=38.58 I/Sig=37.13
Corrections: Lorentz:6.2378 Polar:0.985 LP:0.1627 Incidence:1.0 Final:0.1627
Corrected: Rnet=3057.38 Sigma=82.33 newSigma=215.74
nr h k l QVP DetH DetV Rot Int sigPois PQ obxXyYzZ
3 -19 12 -5 52.28 66.17 25.19 3057.4 215.7 38.6 ........
Waiting 5.0 seconds 4 -25 -2 -4 -7.53 124.92 25.07 3130.2 166.3 19.2 ........
Orig: hor=-50.13 ver=62.85 rot=25.01 hkl: -50.13 62.85 25.01 diff: 0.0 0.0 0.0
generated 125 neighbours tested 6
Frame: 3117.01 3129.05 3124.62 3076.21 3035.94
Theta:4.75 Resolution: 5.11 Chi:38.42 Duration:1.28
Contour: H(-50.65,-49.58)=1.07[7] V(62.42,63.34)=0.92[6] R(-1.43,0.45)=1.88[2]
Pixels: Peak=64/5.7% Surface=104 Bg=1022
Excluded: 39 HV=27/25.96% I(Ex/Pk)=6.91% I(HV/Pk)=5.73% BadI 2.47%
Background: A=1.09 B=1.12 C=3076.7 Sig=78.14 Slope=0.4
Intensity: Hor=255888.94 Ver=257016.38 Rot=261022.67 Plane=260035.98 BgQual=0.02 (peakbg=259933.16)
Shifts:2 H 0.11px 0.02mm V 0.18px 0.03mm rot=-0.1 Frames=2 dxfactor=1.00013 AlphaCorrection: 0.0 0.0 0.0
RotCorrection: 0.0 0.0 0.1
Final Position: -50.12 62.88 24.91 Integrated Position: -50.12 62.88 25.01
Rnet=260035.98 Poisson=806.72 (sigBPB=685.88) GarbageSigma=6425.67 Weight=625.1 PQ=415.99 I/Sig=322.34
Corrections: Lorentz:6.5549 Polar:0.9864 LP:0.1547 Incidence:1.0 Final:0.1547
Corrected: Rnet=40219.25 Sigma=124.77 newSigma=993.85
nr h k l QVP DetH DetV Rot Int sigPois PQ obxXyYzZ
5 -8 -12 0 -50.12 62.88 24.91 40219.3 993.8 416.0 ........
Waiting 5.0 seconds 6 23 8 9 19.20-144.96 25.04 418.8 145.9 2.9 .B......
Orig: hor=31.63 ver=91.37 rot=25.01 hkl: 31.63 91.37 25.01 diff: 0.0 0.0 0.0
generated 125 neighbours tested 26
Frame: 3302.16 3345.22 3347.5 3325.5 3317.96
Theta:5.69 Resolution: 4.27 Chi:-19.0 Duration:1.06
Contour: H(31.06,32.29)=1.23[8] V(90.97,91.83)=0.86[6] R(-1.39,0.41)=1.81[2]
Pixels: Peak=72/6.4% Surface=116 Bg=1046
Excluded: 7 HV=4 Rot=1 I(Ex/Pk)=3.53% BadI 2.31%
Background: A=0.02 B=-2.55 C=3345.89 Sig=83.74 Slope=0.43
Intensity: Hor=57117.98 Ver=56447.85 Rot=61909.0 Plane=59935.32 BgQual=0.09 (peakbg=60085.11)
Shifts:2 H 0.3px 0.04mm V 0.16px 0.02mm rot=0.16 Frames=2 dxfactor=1.00037 AlphaCorrection: 0.0 0.0 0.0
RotCorrection: 0.0 0.0 -0.16
Final Position: 31.67 91.4 25.17 Integrated Position: 31.67 91.4 25.01
Rnet=59935.32 Poisson=751.55 (sigBPB=562.06) GarbageSigma=1385.15 Weight=710.56 PQ=84.35 I/Sig=79.75
Corrections: Lorentz:4.5372 Polar:0.9805 LP:0.2248 Incidence:1.0 Final:0.2248
Corrected: Rnet=13472.79 Sigma=168.94 newSigma=311.37
nr h k l QVP DetH DetV Rot Int sigPois PQ obxXyYzZ
7 -22 7 -5 31.67 91.40 25.17 13472.8 311.4 84.3 ........
Waiting 5.0 seconds Orig: hor=-50.86 ver=96.63 rot=25.01 hkl: -50.86 96.63 25.01 diff: 0.0 0.0 0.0
generated 125 neighbours tested 32
Frame: 3289.4 3301.12 3318.79 3306.18 3296.25
Theta:6.41 Resolution: 3.79 Chi:27.57 Duration:1.14
Contour: H(-51.45,-50.2)=1.25[8] V(96.25,97.19)=0.94[6] R(-1.41,0.42)=1.83[2]
Pixels: Peak=80/7.1% Surface=124 Bg=1034
Excluded: 11 HV=7/5.65% I(Ex/Pk)=2.57% I(HV/Pk)=3.24% BadI 4.86%
Background: A=-0.11 B=2.18 C=3284.93 Sig=63.53 Slope=0.5
Intensity: Hor=51929.97 Ver=52811.41 Rot=56696.33 Plane=53782.92 BgQual=0.09 (peakbg=53628.62)
Shifts:3 H 0.23px 0.04mm V 0.58px 0.09mm rot=0.02 Frames=2 dxfactor=1.00054 AlphaCorrection: 0.0 0.0 0.0
RotCorrection: 0.0 0.0 -0.02
Final Position: -50.83 96.72 25.03 Integrated Position: -50.83 96.72 25.01
Rnet=53782.92 Poisson=613.74 (sigBPB=581.68) GarbageSigma=2613.68 Weight=568.24 PQ=94.65 I/Sig=87.63
Corrections: Lorentz:4.3106 Polar:0.9754 LP:0.2378 Incidence:1.0 Final:0.2378
Corrected: Rnet=12791.91 Sigma=145.97 newSigma=621.65
nr h k l QVP DetH DetV Rot Int sigPois PQ obxXyYzZ
8 -15 -12 -1 -50.83 96.72 25.03 12791.9 621.6 94.6 ........
Waiting 5.0 seconds Orig: hor=69.25 ver=81.52 rot=25.01 hkl: 69.25 81.52 25.01 diff: 0.0 0.0 0.0
generated 125 neighbours tested 14
Frame: 3378.4 3403.81 3406.16 3377.59 3347.56
Theta:6.28 Resolution: 3.87 Chi:-40.06 Duration:1.32
Contour: H(68.7,69.88)=1.18[8] V(80.98,82.06)=1.08[7] R(-1.44,0.45)=1.89[2]
Pixels: Peak=76/6.8% Surface=118 Bg=1030
Excluded: 19 HV=12/10.17% I(Ex/Pk)=10.31% I(HV/Pk)=7.7% BadI 5.03%
Background: A=2.78 B=4.47 C=3322.82 Sig=70.12 Slope=1.45
Intensity: Hor=78954.77 Ver=79425.55 Rot=83207.66 Plane=82018.52 BgQual=0.05 (peakbg=81996.64)
Shifts:2 H 0.31px 0.05mm V 0.04px 0.01mm rot=0.22 Frames=2 dxfactor=1.00031 AlphaCorrection: 0.0 0.0 0.0
RotCorrection: 0.0 0.0 -0.22
Final Position: 69.29 81.52 25.22 Integrated Position: 69.29 81.52 25.01
Rnet=82018.52 Poisson=675.09 (sigBPB=598.25) GarbageSigma=4121.94 Weight=611.33 PQ=134.16 I/Sig=121.49
Corrections: Lorentz:5.1088 Polar:0.9763 LP:0.2005 Incidence:1.0 Final:0.2005
Corrected: Rnet=16443.45 Sigma=135.35 newSigma=826.39
nr h k l QVP DetH DetV Rot Int sigPois PQ obxXyYzZ
9 -24 16 -6 69.29 81.52 25.22 16443.5 826.4 134.2 ........
Waiting 5.0 seconds
Refl nr [10]
exit
s01f002.shoe.Z closed after 57344 bytes 844 lines
Initial shifts 0.0 mm 0.0 mm 0.0 degr.
9 mean shifts [abs] after 6(hv) 6(rot) refls: 0.02[0.03] 0.03[0.03] 0.06[0.13]
dxfactor 1.00025 --> 1.00025
Minimum shifts:0.0 0.0 -0.11 Maximum shifts:0.05 0.09 0.22
9 input, one bad background, 2 Weak, 6 Observed, no output
9 reflections processed in 00:00:00 CPU.
evalccd ended at 19-Sep-2007 23:13:31 CPU time used 00:00:00